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Tank Headspace Monitoring Systems – THMS

Applications

in the Oil and Gas industry.

Water treatment plant in refineries and other oil and gas processes requires the use of tank for storage purposes and as part of the wastewater management plan. The composition of the air confined in the tank headspace provides a good indication of the level of contamination in the wastewater influents. Monitoring gas in tank headspaces also becomes mandatory when it comes to managing oils contaminated water. Explosion risks but also the corrosion and degradation factor are controlled with the blanketing whose automation can largely be optimised by the online measurement of gas concentrations in the headspace. Moreover there is a large number of compounds that will  adduce plant operators detailed information with regards to filtration and decantation processes.

Tank Blanketing Automation

Tank blanketing is the process of filling the headspace in storage vessels and reactors with an inert gas, usually to protect its contents from exploding, degrade but also to protect equipment from corrosion. As oxygen and moisture in the air can be undesired in numerous processes and applications, blanketing is done in a wide range of industries, varying from petrochemicals to food and beverage, pharmaceutical to pure water. Inerting is done for similar reasons but is not limited to storage tanks and reactors only. Any confined space can be sparged with an inert gas to create the desired atmosphere. This ranges from packing food under protective atmosphere to increase shelf life to lowering the oxygen concentration in rooms where welding takes place to reduce risk of fire.

Risks Management

Wrongly engineered or poorly maintained blanketing systems may lead to serious incidents, degraded plant operations and pollution events. A malfunctioning may cause the tank to implode or causes the leaking of air into the tank, which, as mentioned, can have consequences with regard to product quality and, depending on the stored product, can seriously increase risk of explosion.

One way to increase safety and reduce the use of blanketing gas (nitrogen, air…) simultaneously is to control inertisation as a function of gas concentration in the headspace. Depending on the product and the reason for blanketing and inerting, there are tolerances when it comes down to the maximum allowable oxygen, VOCs or other combustibles concentration. Certain monomers require zero percent oxygen to prevent polymerization. Others require a small amount of oxygen for the same reason. In the case of explosion protection, the oxygen concentration does not necessarily need to be zero. In fact for all solvents a so called limiting oxygen concentration exists. Below this concentration there is no risk of explosion. It is obvious that controlling the tank headspace purge based on the concentration will seriously cut nitrogen or other blanketing gas costs. Furthermore the measurement of gas concentrations in the tank headspace provides an important safety parameter.   Thresholds such as Limiting Oxygen Concentration (LOC), Maximum Oxygen Concentration (MOC), Lower Explosive Limit (LEL) indicate application and gas specific limits in terms of concentration.

For example, two threshold values are established for the oxygen concentration in the tank headspace, well below the Limiting Oxygen Concentration; the Lower Intervention Level and the Upper Intervention Level. These two threshold values are the set-points that control the purging sequences. The moment the oxygen concentration reaches the Lower Intervention Limit, the nitrogen flow is intermittent. Purging of the vessel is resumed when the upper intervention limit is exceeded. This means that the inerting system keeps the consumption of nitrogen minimal while safe operation is ensured.

Analyser solutions

Depending on individual process conditions and solvent; O2, H2O and LEL are usually the main parameters of interest. However when odour control is implemented NH3, H2S and VOCs can be added to the monitored parameters.

To meet the needs of the waste recycling facilities, AquaGas offers a unique fully automatic solution for realtime measurement of gas concentrations in Tank Headspaces. AquaGas THMS features the association of a MAMOS multigas analyser fitted with a combination of 9 gas proprietary measuring cells with a field proven, robust and dedicated Exproof sampling train. The system can be multiplexed for controlling up to 4 tank headspaces. Both the gas sampling probe located at the top of the tank and the sample line are temperature controlled above the gas dew point. Depending on the application, the gas can also be fitted with the optional backflush, temperature sensor, insitu filter… The onboard PLC offers a large panel of IOs as required to handle blanketing regulator, breathing valve, safety relief valve…

The THMS is integrated in Australia by AquaGas for continuous and simultaneous measurement of VOC, NH3, CO, CO2, LEL, CxHy, H2S and O2 inside tank headspaces.

Advantages of AquaGas THMS

The AquaGas THMS is a cost efficient and safe solution available in a compact wall mount IP56 enclosure that totally eliminates the need for multiple sensors and probes. The sampling probe can be mounted directly into the vessel or blanketing gas discharge piping and is rated for high dust, moisture or solvents loads. A retractable filter assembly allows cleaning of the sampling probe without the need for dismounting the probe from its matching flange. Zero calibration is performed automatically on a daily basis while span gas calibration is only required quarterly. In very critical applications, the system can be equipped with redundant probes and or sensors for additional safety and self check purposes. Compared to traditional analyser technology, the AquaGas THMS is available at only a fraction of the costs. The most valued perceived benefit however is the significant increase of safety, enormous savings on tank maintenance as well as the optimised process operations.

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Integrated Systems and Customised Services

For better environmental performances.

  • ONLINE WATER ANALYSERS

    Ammonium, Free or Total Chlorine, Hydrazine, Morphine, Phenol, Sulfates, Colour, Silica, Phosphates (Orthophosphates), Hardness, Aluminium, Chromium VI, Iron, Nickel, Lead, Zinc, TH, Alkalinity, Chlorides, Cyanides, Fluorides, Peracetic acid VFA, CaM…

    SERES® online water quality analyser offers multiple sensor and method configurations. Here are the typical  measuring parameter calibrated on the TOPAZ unit. For other parameters or different measuring ranges (MR), please consult us.

  • EMISSIONS AND PROCESS GAS ANALYSERS

    NO, NO2, NOx, SO2, CO, HCl, CO2, H2O, H2S, NH3, N2O, COS, SO3, CH4, HF, HCN, H2…
    Our strong partnerships implemented with world leading CEMS and Process gas analyser manufacturers as well as local distributors,  provide AquaGas with an extensive range of technologies, diverse measuring principle and sampling methods to design and build cost effective, versatile and high performance systems composed of instruments specifically selected  in consideration of the applications.

  • DATA ACQUISITION AND REPORTING SOFTWARE

    Data Aquisition Software (CDAS) is a fully MCERTS accredited (parts A, B, C1 & C2) real time data acquisition software – now available for touch screens and windows 10. CDAS is customisable and flexible, allowing it to collect raw data from a range of instruments for CEMS

  • ISOKINETIC SAMPLING CONSOLE

    Isokinetic sampler developed for short to medium term emissions monitoring, fulfilling all the requirements of the dioxins and persistent organic compounds (POPs), PCBs, metals, HCB and fine dust measurement standard within the same sampling train

  • PORTABLE GAS ANALYSERS

    O2, CO, CO2, NO, NO2, SO2, H2S, H2, CL2, N2O and VOCs

    Professional flue gas analyser combining high quality of sample conditioning with great measurement accuracy for continuous emissions monitoring or online process measurement of up to 9 gases simultaneously.

AquaFID THC CEMS – Continuous Emissions Monitoring Systems

AquaGas supplies four AquaFID THC CEMS

For Sydney’s greater remediation project

AquaGas Monitoring Systems is proud to be part of a major remediation project taking place in the heart of Sydney’s next financial, tourist, cultural and entertainment precinct. This significantly large remediation project is now underway over the next three years to remediate on site 150,000 tonnes of contaminated fill material from a former gas plant.

One of the main actors in this project,  South Pacific market leader for the containment and filtration of hydrocarbons (sheen, gasoline, diesel and oils) and a range of other chemicals, has selected AquaGas Pty Ltd for the supply, installation and commissioning of the Continuous Emissions Monitoring Systems and Process Analysers at the remediation site.

To meet our client environmental monitoring requirements, AquaGas has offered a unique CEMS (Continuous Emissions Monitoring Systems) solution based on Gas Chromatography, the AquaFID. The AquaFID is a fully automatic THC CEMS integrated in Australia by AquaGas for continuous and simultaneous measurement of Total Hydrocarbons (THC), Non Methane Hydrocarbons (NMHC) and Methane (CH4).

The AquaFID key features includes the association of a field proven, robust fast loop heated sampling system from Ankersmid Sampling BVBA (Belgium) with a highly accurate M529H FID analysers from PCF (Italia).

The Exproof sampling system is fitted with extensive features such as calibration port as per international CEMS code and EN14181 for reliable continuous compliance monitoring.

The remediation projects are being strictly monitored in real time. Data is regularly reported to the EPA.

AquaGas Pty Ltd

Integrated systems and Customised Services

aquagas_logo_500px

AquaGas Pty Ltd has the tools and technologies needed to accurately measure atmospheric emissions of gaseous pollutants helping you in improving air quality and environmental performances.


  • Portable Gas Analysers

    Multigas analysers fitted with a combination of proprietary gas cells for short term monitoring of biogas, syngas and combustion processes.

  • Isokinetic Sampling Console

    Isokinetic sampler developed for short to medium term emissions monitoring, fulfilling all the requirements of the dioxins and persistent organic compounds (POPs), PCBs, metals, HCB and fine dust measurement standard within the same sampling train

  • Data Acquisition and reporting Software

    Data Aquisition Software (CDAS) is a fully MCERTS accredited (parts A, B, C1 & C2) real time data acquisition software – now available for touch screens and windows 10. CDAS is customisable and flexible, allowing it to collect raw data from a range of instruments for CEMS

ENVIRONMENTAL MONITORING

Stack Testing

Ankersmid Sampling

APS Portable Gas Sampling System

The emission of pollutants resulting from a multitude of activities (industry, transport, …) alters the atmospheric composition and degrade air quality. Control of gaseous pollutant emissions in the atmosphere has become a major challenge for the protection of human health and the environment. To avoid these risks, the regulation has established discharge limits thresholds for certain pollutants and requires periodic inspections whose frequency depends on the type of activity (from 3 months to 3 years). Accredited stack testing companies are responsible for conducting short to medium term environmental compliance monitoring tasks in a wide range of industries and processes such as power plants and large manufacturing facilities including paper mill, foundry, waste recycling facilities,  refineries…

Prior to be analysed, the gas extracted from the discharge stack or process duct requires delicate conditioning which mainly consist of particulate filtration and moisture removal. Failure to achieve an efficient sample preparation can results in inaccurate measurements, loss of data or damaged equipment.

While stack testers and local authorities are continuously devoting time and knowledge to optimise the methods and protocols related to short to medium terms mandatory analysis campaign, ANKERSMID® has invested its long time expertise in developing the APS Portable Gas Conditioning Systems in direct collaboration with  leading stack testing companies.

As a result, ANKERSMID® Portable Sampling System APS provides stack testers with  features tailored to short term source testing in a robust and light weight design. The complete systems responds to today’s demand in terms of operation and compliance.

ANKERSMID®

Portable Sampling System APS

ANKERSMID® Portable Sampling System APS is a complete gas sampling train composed of:

  • APP Heated Gas Sampling probe

    High temperature filtration

  • AHL Heated Gas Sample line

    Fast and reliable sample gas transfer

  • APS Gas Sampling System

    Accurate and performant gas conditioning

APP Portable Heated Gas Sampling Probe

The APP Heated Gas Sampling Probe is a light weight sampling gun enabling high temperature filtration directly at the sampling point.

Portable probe APP trans 2

The probe is heated up to 180°C in order to maintain the sample temperature above acid gases dew point. A filter element of 150 mm is integrated, suitable for most applications up to 1g of dust per cubic meter of emissions. Thanks to its design, the filter can be replaced or checked without the need of dismounting the probe. For applications where the dust load reaches 10 g/m³, a blow-back option can be fitted. Calibration gas can be injected directly into the probe through the calibration gas port according to emission monitoring standards enforcing test gas feeding via the probe’s filter element.

MAIN FEATURES

180°C operating temperature

Integrated over temperature safety switch

Low temperature alarm contact

Test gas port according to EN14181 available as standard

Light weight

Ready to operate in 15 minutes

Low and Easy maintenance

Universal mounting clamp for heated line

Compact design and universal applicability, easy handling with mounting eye on housing (2m chain incl.)

APP150 Portable heavy duty ABS case for safe transport

AHL Heated Sample Line

AHL Heatedline-v2

The AHL Heated sample line is perfectly suited to mobile applications. It features a highly flexible smooth silicon outer jacket and can be fitted with options enabling efficient installation and operation:

  • Quick connect fittings at both ends: stainless steel pressure release connector directly inserted into the heated lines hard cap terminations (no cold spot)
  • Built-in cable with plugs to feed the APP sampling probe with power – No additional cable or power source required at the sampling location.
  • Additional inner tubes for test gas (calibration via probe filter) or compressed air (back-flush)

APS Portable Gas Conditioning System

 

portable conditioning 3xx 2

The APS portable sampling system is designed so that detailed gas analysis can be carried out at any time in any place. The entire sampling system is housed in a compact and robust carrying case which ensures safe transport and easy set-up. All the components can be easily accessed for inspection or routine maintenance. The APS concept allows you to perform gas analysis in an efficient manner, safely and with a minimum of maintenance. This system ensures reliable sample preparation without loss and prevents damage on the downstream analysis system. It is suitable for a large range of applications and has already been adopted by many stack testers around the world.

MAIN FEATURES

Fully automated

Moisture alarm (detection of sample condensates)

Extremely stable dew point +/-1 degree C

Optimal reliability

Compact and robust design

Light weight

Ready to operate in 15 minutes

Low and Easy maintenance

PFA coated heat exchanger

PTFE coated sampling pump

Preliminary sample filter

Built-in temperature controller for the heated line

AquaGas Pty Ltd

Integrated high performance monitoring solutions

aquagas_logo_500px

AquaGas Pty Ltd has the tools and technologies needed to accurately measure atmospheric emissions of gaseous pollutants helping you in improving air quality and environmental performances.

  • Portable Gas Analysers

    Multigas analysers fitted with a combination of proprietary gas cells for short term monitoring of biogas, syngas and combustion processes.

  • Isokinetic Sampling Console

    Isokinetic sampler developed for short to medium term emissions monitoring, fulfilling all the requirements of the dioxins and persistent organic compounds (POPs), PCBs, metals, HCB and fine dust measurement standard within the same sampling train

  • Data Acquisition and reporting Software

    Data Aquisition Software (CDAS) is a fully MCERTS accredited (parts A, B, C1 & C2) real time data acquisition software – now available for touch screens and windows 10. CDAS is customisable and flexible, allowing it to collect raw data from a range of instruments for CEMS

 

Ankersmid Sampling

ANKERSMID® , well-known in the monitoring industry as Ankersmid M&C, has the benefits of 30 years of experience in developing state of the art gas sampling and gas conditioning equipment tailored to CEMS (Continuous Emissions Monitoring Systems) and stack testing (short to medium term measurements). Subsidiaries in several countries (Netherlands, France, China, Roumania, Germany, Korea…) and more than 100 employees world-wide place ANKERSMID® in a leading position within the field of environmental monitoring and process control instrumentation.